ORGANIC-PHARMACEUTICALS LITERATURE
Schmidt, M. U., et al. "Electron Diffraction, X-Ray Powder Diffraction and Pair-Distribution- Function Analyses to Determine the Crystal Structures of Pigment Yellow 213, C23H21N5O9." Acta Crystallographica Section B: Structural Science, vol. 65, no. 2, pp. 189–99,, 2009, doi: 10.1107/S0108768109003759
Gorelik, T., et al. "Using Electron Diffraction to Solve the Crystal Structure of a Laked Azo Pigment." Crystal Growth and Design, vol. 9, no. 9, pp. 3898–903, 2009, doi: 10.1021/cg801099r
Gorelik, T., et al. "H-Bonding Schemes of Di-and Tri-p-Benzamides Assessed by a Combination of Electron Diffraction, X-Ray Powder Diffraction and Solid-State NMR." CrystEngComm, vol. 12, no. 6, pp. 1824–32, 2010, doi: 10.1039/b920569a
Kolb, U., et al. "Structural Characterization of Organics Using Manual and Automated Electron Diffraction." Polymer Reviews, vol. 50, no. 3, pp. 385–409, 2010, doi: 10.1080/15583724.2010.494238
Gorelik, T. E., et al. "Ab-Initio Crystal Structure Analysis and Refinement Approaches of Oligo p-Benzamides Based on Electron Diffraction Data." Acta Crystallographica Section B: Structural Science, vol. 68, no. 2, International Union of Crystallography, pp. 171–81, 2012, doi: 10.1107/S0108768112003138
Gorelik, T. E., et al. "Detecting Crystalline Nonequilibrium Phases on the Nanometer Scale." Crystal Growth and Design, vol. 12, no. 6, pp. 3239–42, 2012, doi: 10.1021/cg300377j
Virginia Altoe, et al. "Electron Microscopy Reveals Structure and Morphology of One Molecule Thin Organic Films", 2012, doi: https://doi.org/10.1021/nl203776n
Förster, C., et al. "Crystalline Non-Equilibrium Phase of a Cobalt(II) Complex with Tridentate Ligands." European Journal of Inorganic Chemistry, vol. no. 6, pp.920–24, 2015, doi: 10.1002/ejic.201403200
Van Genderen, E., et al. "Ab Initio Structure Determination of Nanocrystals of Organic Pharmaceutical Compounds by Electron Diffraction at Room Temperature Using a Timepix Quantum Area Direct Electron Detector." Acta Crystallographica Section A: Foundations and Advances, vol. 72, International Union of Crystallography, pp.236–42, 2016, doi: 10.1107/S2053273315022500
Gorelik, T. E., et al. "Crystal Structure of Disordered Nanocrystalline _II-Quinacridone Determined by Electron Diffraction." CrystEngComm, vol. 18, no. 4, Royal Society of Chemistry, pp. 529–35, 2016, doi: 10.1039/c5ce01855b
Wilke, M., et al. "The Crystallisation of Copper(II) Phenylphosphonates." Dalton Transactions, vol. 45, no. 43, Royal Society of Chemistry, pp. 17453–63, 2016, doi: 10.1039/c6dt02904c
Wang, Y., et al. "Elucidation of the Elusive Structure and Formula of the Active Pharmaceutical Ingredient Bismuth Subgallate by Continuous Rotation Electron Diffraction." Chemical Communications, vol. 53, no. 52, pp. 7018–21, 2017, doi: 10.1039/c7cc03180g
Das, P. P., et al. "Crystal Structures of Two Important Pharmaceuticals Solved by 3D Precession Electron Diffraction Tomography." Organic Process Research and Development, vol. 22, no. 10, American Chemical Society, pp. 1365–72, 2018, doi: 10.1021/acs.oprd.8b00149
Gruene, T., et al. "Rapid Structure Determination of Microcrystalline Molecular Compounds Using Electron Diffraction." Angewandte Chemie – International Edition, vol. 57, no. 50, pp. 16313–17, 2018, doi: 10.1002/anie.201811318
Jones, C. G., et al. "The CryoEM Method MicroED as a Powerful Tool for Small Molecule Structure Determination." ACS Central Science, vol. 4, no. 11, pp. 1587–92, 2018, doi: 10.1021/acscentsci.8b00760
Kunde, T., et al. "Microcrystal Electron Diffraction (MicroED) for Small-Molecule Structure Determination." Angewandte Chemie – International Edition, vol. 58, no. 3,pp.666–68, 2019, doi: 10.1002/anie.201813215
Clabbers, M. T. B., et al. "Reducing Dynamical Electron Scattering Reveals Hydrogen Atoms." Acta Crystallographica Section A: Foundations and Advances, vol. 75, no. 1, International Union of Crystallography, pp. 82–93, 2019, doi: 10.1107/S2053273318013918
Jones, C. G., et al. "Characterization of Reactive Organometallic Species via MicroED." ACS Central Science, vol. 5, no. 9, pp. 1507–13, 2019, doi: 10.1021/acscentsci.9b00403
Andrusenko, I., et al. "The Crystal Structure of Orthocetamol Solved by 3D Electron Diffraction." Angewandte Chemie – International Edition, vol. 58, no. 32, pp.10919–22, 2019, doi: 10.1002/anie.201904564
Guzmán-Afonso, C., et al. "Understanding Hydrogen-Bonding Structures of Molecular Crystals via Electron and NMR Nanocrystallography." Nature Communications, vol. 10, no. 1, Springer US, pp. 1–10, 2019, doi: 10.1038/s41467-019-11469-2
Broadhurst, E. T., et al. "Polymorph Evolution during Crystal Growth Studied by 3D Electron Diffraction." IUCrJ, vol. 7, pp. 5–9, 2020, doi: 10.1107/S2052252519016105
Gemmi, M., et al. "A New Method Based on Electron Diffraction for Detecting Nanoparticles in Injectable Medicines." Journal of Pharmaceutical Sciences, vol. 109, no. 1, Elsevier Ltd, pp. 891–99, 2020, doi: 10.1016/j.xphs.2019.07.008
Iryna Andrusenko, et al. "A new olanzapine cocrystal obtained from volatile deep eutectic solvents and determined by 3D electron diffraction", Acta Cryst. . B76, 1036–1044, 2020, doi: 10.1107/S2052520620012779
Victoria Hamilton, et al. "Racemic Conglomerate Formation via Crystallization of Metaxalone from Volatile Deep Eutectic Solvents", Cryst. Growth Des. 20, 4731_4739, 2020, doi: 10.1021/acs.cgd.0c00497
Emma Danelius, et al. "MicroED in natural product and small molecule research", The Royal Society of Chemistry, 2020, doi: 10.1039/d0np00035c
Bo Wang, et al. "Absolute configuration determination of pharmaceutical crystalline powders by MicroED via chiral salt formation", 2022, doi: https://doi.org/10.1039/d2cc00221c
Nicole Hoefer, et al. "Crystal Structure Determination of Gramicidin by Microcrystal Electron Diffraction", 2022, doi: https://doi.org/10.1017/S1431927622004573
Tatiana E. Gorelik, et al. "Crystal structure of natural product argyrin-D determined by 3D electron diffraction", 2022, doi: https://doi.org/10.1039/D2CE00707J
Lightowler, et al. "Investigating polymorphism in small molecules using three-dimensional electron diffraction", 2022, doi: https://su.diva-portal.org/smash/record.jsf?pid=diva2%3A1685658
Laurence R. Doyle, et al. "MicroED characterization of a robust cationic σ-alkane complex stabilized by the [B(3,5-(SF5)2C6H3)4]− anion, via on-grid solid/gas single-crystal to single-crystal reactivity", 2022, doi: https://doi.org/10.1039/D2DT00335J
Vince M. Hipwell, et al. "Scale-Dependent Photosalience and Topotactic Reaction of Microcrystalline Benzylidenebutyrolactone Determined by Electron Microscopy and Electron Diffraction", 2022, doi: https://doi.org/10.1021/acs.cgd.1c01378
E. Mugnaioli, et al. "Strategies for structure solution of small-molecule organics by 3D ED using a small beam", 2022, doi: https://journals.iucr.org/a/issues/2021/a2/00/a59751/a59751.pdf
S. Plana-Ruiz, et al. "The crystal structure determination of an organic dye with triclinic symmetry by electron diffraction", 2022, doi: https://doi.org/10.1107/S0108767321095234
Darpandeep Aulakh, et al. "Retrospect and Prospect of Small Molecule Microcrystal Electron Diffraction for Pharmaceutical Industry", 2022, doi: https://journals.iucr.org/a/issues/2022/a1/00/a60899/a60899.pdf
Iryna Andrusenko, et al. "3D electron diffraction for structure determination of small-molecule nanocrystals: A possible breakthrough for the pharmaceutical industry", 2022, doi: https://doi.org/10.1002/wnan.1810
Christopher J. H. Smalley, et al. "A structure determination protocol based on combined analysis of 3D-ED data, powder XRD data, solid-state NMR data and DFT-D calculations reveals the structure of a new polymorph of l-tyrosine", 2022, doi: https://doi.org/10.1039/D1SC06467C
Shuting Li, et al. "Direct Structure determination from Spherulites using 3D Electron Diffraction", 2022, doi: https://doi.org/10.26434/chemrxiv-2022-jh1lx
Erik Svensson Grape, et al. "Structure of the active pharmaceutical ingredient bismuth subsalicylate", 2022, doi: https://doi.org/10.1038/s41467-022-29566-0
Erik Svensson Grape, et al. "Triple helix and rod structures of the antiseptic drug bibrocathol revealed by electron crystallography", 2022, doi: https://doi.org/10.1039/D2CC04209F
Iryna Andrusenko, et al. "True molecular conformation and structure determination by three-dimensional electron diffraction of PAH by-products potentially useful for electronic applications·, 2022, doi: https://doi.org/10.1107/S205225252201154X
Iryna Andrusenko, et al. "Two New Organic Co-Crystals Based on Acetamidophenol Molecules", 2022, doi: https://doi.org/10.3390/sym14030431
Joseph Hitchen, et al. "Organic Cocrystals of TCNQ and TCNB Based on an Orthocetamol Backbone Solved by Three-Dimensional Electron Diffraction", 2023, doi: https://doi.org/10.1021/acs.cgd.1c01095
Kiyofumi Takaba, et al. "Comprehensive application of XFEL micro crystallography for novel organic compounds", 2023, doi: https://doi.org/10.26434/chemrxiv-2023-69p99
Tatiana E. Gorelik, et al. "Crystal structure of 9, 10-bis-((perchloro-phenyl)-ethynyl) anthracene determined from three-dimensional electron diffraction data", 2023, doi: https://doi.org/10.1515/zkri-2023-0009
Danelius E, et al. "MicroED as a powerful tool for structure determination of macrocyclic drug compounds directly from their powder formulations", 2023, doi: https://doi.org/10.1101/2023.07.31.551405
Joseph Hitchen, et al. "Organic Cocrystals of TCNQ and TCNB Based on an Orthocetamol Backbone Solved by Three-Dimensional Electron Diffraction", 2023, doi: https://doi.org/10.1021/acs.cgd.1c01095
Molly Lightowler, et al. "Phase identification and discovery of hidden crystal forms in a polycrystalline pharmaceutical sample using high-throughput 3D electron diffraction", 2023, doi: https://chemrxiv.org/engage/chemrxiv/article-details/6466d172a32ceeff2ddee872
Bu G1, et al. "Polymorphic Structure Determination of the Macrocyclic Drug Paritaprevir by MicroED", 2023, doi: https://doi.org/10.1101/2023.09.09.556999
Jessica E. Burch, et al. "Putting MicroED to the test: an unabridged account of the evaluation of 30 diverse pharma compounds", 2023, doi: https://chemrxiv.org/engage/chemrxiv/article-details/61670e747d3da50c42f692b9
Kunal Kumar Jha, et al. "Structures of Vitamin D derivatives by electron diffraction", 2023, doi: https://programme.conventus.de/en/mc-2023/posters/52cfbada-3556-4038-ab19-40980527ee74
Jieye Lin, et al. "Unraveling the Structure of Meclizine Dihydrochloride with MicroED", 2023, doi: https://doi.org/10.1101/2023.09.05.556418
Pedro Nunes, et al. "3D Electron Diffraction of Small Molecules on the MerlinEM Detector", 2023, doi: https://doi.org/10.1093/micmic/ozad067.511
Lorenza Romagnoli, et al. "4,4′-(Anthracene-9,10-diylbis(ethyne-2,1-diyl))bis(1-methyl-1-pyridinium) Lead Iodide C30H22N2Pb2I6: A Highly Luminescent, Chemically and Thermally Stable One-Dimensional Hybrid Iodoplumbate", 2023, doi: https://doi.org/10.1021/acs.chemmater.2c03798
Tatiana E. Gorelik, et al. "Analysis of diffuse scattering in electron diffraction data for the crystal structure determination of Pigment Orange 13, C32H24Cl2N8O2", 2023, doi: https://doi.org/10.1107/S2052520623000720
Shuting Li, et al. "Direct structure determination of vemurafenib polymorphism from compact spherulites using 3D electron diffraction", 2023, doi: https://doi.org/10.1038/s42004-022-00804-2
Jieye Lin1, et al. "Distinct Conformations of Mirabegron Determined by MicroED", 2023, doi: https://doi.org/10.1101/2023.06.28.546957
Emma Danelius, et al. "MicroED in drug discovery", 2023, doi: https://doi.org/10.1016/j.sbi.2023.102549
Kiyofumi Takaba, et al. "Structural resolution of a small organic molecule by serial X-ray free-electron laser and electron crystallography", 2023, doi: https://doi.org/10.1038/s41557-023-01162-9
Diptajyoti Gogoi, et al. "Structure Elucidation of Olanzapine Molecular Salts by Combining Mechanochemistry and Micro-Electron Diffraction", 2023, doi: https://doi.org/10.1021/acs.cgd.3c00432
Dr. Durga Prasad Karothu, et al. "The Elusive Structure of Levocetirizine Dihydrochloride Determined by Electron Diffraction", 2023, doi: https://doi.org/10.1002/anie.202303761
Bu, Guanhong Wieske, et al. "Simeprevir: The First Macrocyclic Drug Elucidated Ab Initio by MicroED", 2023, doi: https://www.diva-portal.org/smash/record.jsf?pid=diva2%3A1750553&dswid=-8778
Avital Wagner, et al. "Structure Determination of Biogenic Crystals Directly from 3D Electron Diffraction Data", 2024, doi: https://pubs.acs.org/doi/10.1021/acs.cgd.3c01290
Leung, Helen W, et al. "From formulation to structure: 3D electron diffraction for the structure solution of a new indomethacin polymorph from an amorphous solid dispersion", 2024, doi: https://doi.org/10.1107/S2052252524008121
Hidetomo Yokoo, et al. "Rapid Structure Determination of Ranitidine Hydrochloride API in Two Crystal Forms Using Microcrystal Electron Diffraction", 2024, doi: https://doi.org/10.1248/cpb.c23-00745
Agata Jeziorna, et al. "SCXRD, CSP-NMRX and microED in the quest for three elusive polymorphs of meloxicam", 2024, doi: https://doi.org/10.1107/S2052252524011898
Youwei Xu, et al. "Structure Determination and 3D ED/MicroED-Guided Synthesis of a New (S)-Ibuprofen–l-phenylalanine Co-Crystal", 2024, doi: https://doi.org/10.1021/acs.cgd.3c01391
Erik Svensson Grape, et al. "Brilliantly red: the structure of carmine", 2024, doi: https://doi.org/10.26434/chemrxiv-2024-30t84-v2
Emre Yörük, et al. "Electron diffraction unveils the 2D metal-radical framework of two molecule-based magnets", 2024, doi: https://doi.org/10.1039/D4QI02257B
Yaşar Krysiak, et al. "High Temperature Electron Diffraction on Organic Crystals: In Situ Crystal Structure Determination of Pigment Orange 34", 2024, doi: https://doi.org/10.1021/jacs.3c14800
Kaichao Wang, et al. "Large-Scale Synthesis of High-Purity Isoguanosine and Resolution of its Crystal Structure by Microcrystal Electron Diffraction", 2024, doi: https://doi.org/10.1002/open.202400141
Molly Lightowler, et al. "Phase Identification and Discovery of an Elusive Polymorph of Drug-Polymer Inclusion Complex Using Automated 3D Electron Diffraction", 2024, doi: https://doi.org/10.1002/anie.202317695
